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ChemicalBook CAS DataBase List (6-ETHOXYPYRIDIN-3-YL)BORONIC ACID

(6-ETHOXYPYRIDIN-3-YL)BORONIC ACID synthesis

1synthesis methods
-

Yield: 61%

Reaction Conditions:

Stage #1:5-bromo-2-ethoxypyridine with n-butyllithium in diethyl ether;hexane at -78; for 2 h;
Stage #2: with Triisopropyl borate in diethyl ether;hexane at -78; for 2 h;

References:

Parry, Paul R.;Bryce, Martin R.;Tarbit, Brian [Synthesis,2003,# 7,p. 1035 - 1038]

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