2-Ethoxy-3-pyridineboronic acid synthesis
- Product Name:2-Ethoxy-3-pyridineboronic acid
- CAS Number:854373-97-0
- Molecular formula:C7H10BNO3
- Molecular Weight:166.97
14529-53-4
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$5.00/5g
854373-97-0
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$19.00/1g
Yield:854373-97-0 70%
Reaction Conditions:
Stage #1:2-ethoxypyridine with lithium diisopropyl amide in tetrahydrofuran;hexane at -50; for 1 h;
Stage #2: with Triisopropyl borate in tetrahydrofuran;hexane at -50 - -10;
References:
Thompson, Amy E.;Batsanov, Andrei S.;Bryce, Martin R.;Saygili, Nezire;Parry, Paul R.;Tarbit, Brian [Tetrahedron,2005,vol. 61,# 21,p. 5131 - 5135]