6-FLUOROQUINOLINE-4-CARBOXYLIC ACID synthesis
- Product Name:6-FLUOROQUINOLINE-4-CARBOXYLIC ACID
- CAS Number:220844-73-5
- Molecular formula:C10H6FNO2
- Molecular Weight:191.16
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
1000210-73-0
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220844-73-5
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Yield: 98%
Reaction Conditions:
in water at 200; for 3 h;Sealed tube;
Steps:
53 Synthesis of 6-fluoroquinoline-4-carboxylic acid (53B)
53A (0.30g, 1.28mmol) was dissolved in water (8mL), the tube was sealed at 200°C for 3h, the pH was adjusted to 3-4 with dilute hydrochloric acid, and then filtered with suction to obtain 0.24g of dark brown solid with a yield of 98%.
References:
CN113061098, 2021, A Location in patent:Paragraph 0417; 0418; 0421; 0422
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220844-73-5
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220844-73-5
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