ChemicalBook CAS DataBase List 6-Formyl-2,3-dimethoxybenzoic acid

6-Formyl-2,3-dimethoxybenzoic acid synthesis

12synthesis methods

Product Name:6-Formyl-2,3-dimethoxybenzoic acid
CAS Number:519-05-1
Molecular formula:C10H10O5
Molecular Weight:210.18

1521-38-6
288 suppliers
$8.00/10g

519-05-1
59 suppliers
$65.00/500 mg

Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: palladium diacetate; dipotassium hydrogenphosphate / 8 h / 96 °C
2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 4 h / Reflux
3.1: water; potassium hydroxide / 4 h / 40 °C
3.2: 1 h / 5 °C / pH 1 - 2

References:

Li, Jihui;Liu, Yongxiang;Song, Xinjing;Wu, Tianxiao;Meng, Jiaxin;Zheng, Yang;Qin, Qiaohua;Zhao, Dongmei;Cheng, Maosheng [Organic Letters,2019,vol. 21,# 17,p. 7149 - 7153]

569-31-3 Synthesis