6-METHYL-2-HEPTANONE synthesis
- Product Name:6-METHYL-2-HEPTANONE
- CAS Number:928-68-7
- Molecular formula:C8H16O
- Molecular Weight:128.21
110-93-0
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928-68-7
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Yield:928-68-7 97.3%
Reaction Conditions:
with hydrogen;palladium/alumina at 60; under 1500.15 Torr; for 66 h;Product distribution / selectivity;Autoclave;
Steps:
a.5
Step aExamples 1 to 7A 125 mL-autoclave (Hastelloy) was charged with 30 g of MH with a purity of 96.7% and the catalyst as given in table 1. The amount of catalyst was 33.3 mg in all examples. The mixture was heated to 60° C. and hydrogen was added at 2 bar. After reaction, when no up-take of hydrogen was observed any more, the mixture was cooled to 20° C., the catalyst separated by filtration and the mixture analyzed by gas chromatography.
References:
DSM IP ASSETS B.V. US2012/53353, 2012, A1 Location in patent:Page/Page column 4
2009-74-7
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928-68-7
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