ChemicalBook CAS DataBase List 6-phenyldodecane

6-phenyldodecane synthesis

10synthesis methods

Product Name:6-phenyldodecane
CAS Number:2719-62-2
Molecular formula:C18H30
Molecular Weight:246.43

112-52-7
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$7.00/25g

71-43-2
718 suppliers
$11.19/25ML

123-01-3 Synthesis

123-01-3
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$9.00/5g

2719-62-2
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2719-61-1
3 suppliers
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2719-63-3
4 suppliers
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2400-00-2
11 suppliers
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2719-64-4
3 suppliers
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Yield:-

Reaction Conditions:

with 1-butyl-iso-quinolinium hydrogen sulfate;iron(III) chloride at 60; under 2250.23 Torr; for 0.833333 h;Autoclave;Inert atmosphere;Temperature;Reagent/catalyst;

Steps:

2; 12-15 Example 12
General procedure: Catalyst a is used as a catalyst, catalyst a: ionic liquid S1, and the auxiliary agent is zinc chloride.80 g of benzene and 100 g of 1-chlorododecane were added to the reaction vessel, followed by the addition of 18 g of N-(3-sulfonate)propyl-5-sulfonate isoquinoline trifluoromethanesulfonate ionic liquid. 4.5 g of zinc chloride was added. The air in the autoclave was replaced with nitrogen, pressurized to 0.3 MPa, and heated to 30 ° C for 30 min. The amount of the catalyst and the reaction conditions are shown in Table 3. After the end of the reaction, the supernatant liquid was taken for GC-MS analysis, and the results are shown in Table 4. The lower layer was the catalyst phase, and was re-added to the reaction vessel. The above operation was repeated, and the effect of the catalyst was repeated 10 times without significant change.

References:

Sinopec Corporation;Sinopec Corporation Petrochemical Sciences Institute;Wang Jing;Zhao Bin;Shi Junjun;Liang Zhanqiao;Xi Lei;Wang Zhiqiang;Zhu Ning;Ruan Chi;Du Peng CN109721462, 2019, A Location in patent:Paragraph 0080-0088; 0098-0101