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6-(pyridin-4-ylmethoxy)-pyridin-3-ylamine synthesis

2synthesis methods
586-95-8 Synthesis
4-Pyridylcarbinol

586-95-8
358 suppliers
$6.00/1g

6-(pyridin-4-ylmethoxy)-pyridin-3-ylamine

181633-38-5
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: NaH / dimethylformamide / 18 h / -20 - 20 °C
2: SnCl2; conc. HCl / ethanol / 1 h / 50 °C

References:

Bromidge, Steven M.;Davies, Susannah;Duckworth;Forbes, Ian T.;Jones, Graham E.;Jones, Jerome;King, Frank D.;Blackburn, Thomas P.;Holland, Vicky;Kennett, Guy A.;Lightowler, Sean;Middlemiss, Derek N.;Riley, Graham J.;Trail, Brenda;Wood, Martyn D. [Bioorganic and Medicinal Chemistry Letters,2000,vol. 10,# 16,p. 1867 - 1870]