(αS)-α-AMino-benzenebutanoic Acid Methyl Ester Hydrochloride synthesis
- Product Name:(αS)-α-AMino-benzenebutanoic Acid Methyl Ester Hydrochloride
- CAS Number:60425-49-2
- Molecular formula:C11H16ClNO2
- Molecular Weight:229.7032
Yield:60425-49-2 100%
Reaction Conditions:
with hydrogenchloride for 5 h;Heating / reflux;
Steps:
1
To L-Homophe (153 mg, 0.853 mmol) in 10 mL of MeOH was added a solution of HCl in MeOH (3M, 5 ml), and the reaction mixture was heated at reflux for 5 hours. The mixture was evaporated to dryness in vacuo and resulted in a white solid (196 mg, yield: 100%) which was used in the next step without further purification.
References:
US2009/69329,2009,A1 Location in patent:Page/Page column 26
67-56-1
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82795-51-5
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60425-49-2
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$165.00/1g
106860-17-7
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$130.00/50mg
60425-49-2
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$165.00/1g
100-39-0
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60425-49-2
42 suppliers
$165.00/1g