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61133-09-3

Benzeneacetaldehyde, α-hexyl-3,5-dimethoxy-α-methyl- synthesis

2synthesis methods
39192-51-3 Synthesis
1-(3 5-DIMETHOXYPHENYL)HEPTAN-1-ONE  96

39192-51-3
32 suppliers
$67.00/250mg

Benzeneacetaldehyde, α-hexyl-3,5-dimethoxy-α-methyl-

61133-09-3
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-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 1.) n-BuLi / 1.) THF-hexane, -78 deg C, 1 h, 2.) -> RT, then reflux, 3 h
2: 6.7 g / 1.) n-BuI / 1.) THF-hexane, -78 deg C, 2 h, 2.) RT, 2 h

References:

Singh, Vishwakarma;Kane, Vinayak V.;Martin, Arnold R. [Synthetic Communications,1981,vol. 11,# 6,p. 429 - 438]