N-(3-chlorophenyl)-4-(2-chloropyridin-4-yl)-1,3,5-triazin-2-amine synthesis
- Product Name:N-(3-chlorophenyl)-4-(2-chloropyridin-4-yl)-1,3,5-triazin-2-amine
- CAS Number:652153-37-2
- Molecular formula:C14H9Cl2N5
- Molecular Weight:318.16
Yield:652153-37-2 85%
Reaction Conditions:
in isopropyl alcohol at 20;
Steps:
2.f Step f
To a suspension of 6 (256 mg; 1. 1 mmol) in 2-propanol (5 mL) was added 3- chloroaniline (192 UL ; 1. 8 mmol) and the suspension was stirred at room temp overnight. The product was filtered off, washed with 2-propanol and dried. Yield: 305 mg (85%).
References:
WO2004/84634,2004,A1 Location in patent:Page 46
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