13,14-(1,3-Butadiene-1,4-diyl)-[9,10-(1,3-butadiene-1,4-diyl)-[5,6-(1,3-butadiene-1,4-diyl)-[1,2-(1,3-butadiene-1,4-diyl)-4,8,12,16-tetraoxacyclohexadecane-1,5,9,13-tetraene-3,7,11,15-tetraone]]] synthesis
- Product Name:13,14-(1,3-Butadiene-1,4-diyl)-[9,10-(1,3-butadiene-1,4-diyl)-[5,6-(1,3-butadiene-1,4-diyl)-[1,2-(1,3-butadiene-1,4-diyl)-4,8,12,16-tetraoxacyclohexadecane-1,5,9,13-tetraene-3,7,11,15-tetraone]]]
- CAS Number:6543-57-3
- Molecular formula:C28H16O8
- Molecular Weight:480.42
69-72-7
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Yield:6543-57-3 36%
Reaction Conditions:
with trichlorophosphate in toluene; for 6 h;Reflux;
References:
Tanaka, Koichi;Hayashi, Satoshi;Caira, Mino R. [Organic Letters,2008,vol. 10,# 11,p. 2119 - 2122] Location in patent:supporting information; experimental part