Zinc(II)-2,3,9,10,16,17,23,24-octafluoro-29H ,31H - phthalocyanin synthesis
- Product Name:Zinc(II)-2,3,9,10,16,17,23,24-octafluoro-29H ,31H - phthalocyanin
- CAS Number:676519-80-5
- Molecular formula:C32H8F8N8Zn
- Molecular Weight:721.84
134450-56-9
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Yield:676519-80-5 62%
Reaction Conditions:
in further solvent(s);under N2, C6H2F2(CN)2 (4 mmol) and Zn(CH3COO)2 (1.1 mmol) in 1-chloronaphthalene heated for 20 h under reflux, cooled; deluted with MeOH, stirred for 1 h, washed (MeOH, then DMF), ppt. filtered, washed (MeOH), dried at 150°C in vac., purified by sublimation in vac. at 370°C;
References:
Brinkmann;Kelting;Makarov;Tsaryova;Schnurpfeil;Woehrle;Schlettwein [Physica Status Solidi (A) Applications and Materials,2008,vol. 205,# 3,p. 409 - 420]
134450-56-9
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$40.00/500mg
7646-85-7
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$10.00/25ml
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