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ChemicalBook CAS DataBase List 7-bromo-9,9-dihexylfluoren-2-yl-boronic acid
934762-26-2

7-bromo-9,9-dihexylfluoren-2-yl-boronic acid synthesis

3synthesis methods
-

Yield:934762-26-2 52%

Reaction Conditions:

Stage #1: 2,7-dibromo-9,9-di-n-hexylfluorenewith n-butyllithium in hexane;
Stage #2: in hexane;
Stage #3: with hydrogenchloride in hexane;water at -78;

References:

Sun, Han-Sheng;Lee, Chia-Hao;Lai, Chia-Sheng;Chen, Hsin-Lung;Tung, Shih-Huang;Chen, Wen-Chang [Soft Matter,2011,vol. 7,# 9,p. 4198 - 4206] Location in patent:experimental part