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ChemicalBook CAS DataBase List 1-BroMo-4-(1,1-diMethylheptyl)-2-(phenylMethoxy)-benzene
70120-16-0

1-BroMo-4-(1,1-diMethylheptyl)-2-(phenylMethoxy)-benzene synthesis

7synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 78 percent / H2 / 10percent Pd/C / ethanol / 13 h / 2585.7 Torr
2: 100 percent / Br2 / CCl4 / 0.25 h / 30 °C
3: 1.) KH / 1.) DMF, -18 deg C, 15 min, 2.) 25 deg C, 30 min

References:

Melvin, Lawrence S.;Johnson, M. Ross;Harbert, Charles A.;Milne, George M.;Weissman, Albert [Journal of Medicinal Chemistry,1984,vol. 27,# 1,p. 67 - 71]