
ethyl 7-methoxy-4-oxo-1,4-dihydroquinoline-3-carboxylate synthesis
- Product Name:ethyl 7-methoxy-4-oxo-1,4-dihydroquinoline-3-carboxylate
- CAS Number:71083-05-1
- Molecular formula:C13H13NO4
- Molecular Weight:247.25
![2-[(3-METHOXYPHENYLAMINO)-METHYLENE]MALONIC ACID DIETHYL ESTER](/CAS/GIF/56881-19-7.gif)
56881-19-7
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71083-05-1
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Yield: 40%
Reaction Conditions:
for 10 h;
Steps:
4.2.3 General procedure for synthesis of 28-39
General procedure: A solution of compound 16-27 (7.36mmol) in 14 diphenylether (50mL) was heated at 250°C for 10h. After cooling, precipitated solid was separated by filtration, washed with diethylether. The residue was dried under reduced pressure to give corresponding 15 quinolone 28-39.
References:
Mori, Shuichi;Iinuma, Hiroto;Manaka, Noriaki;Ishigami-Yuasa, Mari;Murayama, Takashi;Nishijima, Yoshiaki;Sakurai, Akiko;Arai, Ryota;Kurebayashi, Nagomi;Sakurai, Takashi;Kagechika, Hiroyuki [European Journal of Medicinal Chemistry,2019,vol. 179,p. 837 - 848]

536-90-3
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71083-05-1
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87-13-8
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71083-05-1
26 suppliers
$98.00/1g