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74398-85-9

2-Butenedioic acid, 2-fluoro-, 1,4-dimethyl ester, (2E)- synthesis

3synthesis methods
2-Butenedioic acid, 2-fluoro-, 1,4-dimethyl ester, (2E)-

74398-85-9
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18414-17-0 Synthesis
2-Butenedioic acid, 2-fluoro-, 1,4-dimethyl ester, (2Z)-

18414-17-0
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Yield:18414-17-0 81 % Spectr. ,74398-85-9 19 % Spectr.

Reaction Conditions:

with Amberlyst A 26*dihydrogentrifluoride in tetrachloromethane at 60; for 30 h;Title compound not separated from byproducts;

References:

Cousseau, Jack;Albert, Patrice [Bulletin de la Societe Chimique de France,1986,# 6,p. 910 - 915]