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ChemicalBook CAS DataBase List Ethyl 6-chloro-[1,2,4]triazolo[4,3-b]pyridazine-3-carboxylate
75680-93-2

Ethyl 6-chloro-[1,2,4]triazolo[4,3-b]pyridazine-3-carboxylate synthesis

4synthesis methods
17284-97-8 Synthesis
3-Chloro-6-hydrazinopyridazine

17284-97-8
199 suppliers
$8.00/1g

55896-93-0 Synthesis
Ethyl 2-(Chlorosulfonyl)acetate

55896-93-0
224 suppliers
$26.80/1L

Acetic acid, [[2-(6-chloro-3-pyridazinyl)hydrazino]sulfonyl]-, ethyl ester (9CI)

76195-97-6
0 suppliers
inquiry

Acetic acid, [(6-chloro-3-pyridazinyl)hydrazono]-, ethyl ester

69579-06-2
4 suppliers
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Yield:75680-93-2 500 mg ,76195-97-6 30% ,69579-06-2 150 mg

Reaction Conditions:

with triethylamine in dichloromethane;1.) 10 h., room temp.; 2.) reflux, 2 h.;

References:

Kosary, J.;Sohar, P. [Acta Chimica Academiae Scientiarum Hungaricae,1980,vol. 103,# 4,p. 405 - 414]