3-Bromomethyl-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxy synthesis
- Product Name:3-Bromomethyl-2,5-dihydro-2,2,5,5-tetramethyl-1H-pyrrol-1-yloxy
- CAS Number:76893-32-8
- Molecular formula:C9H15BrNO*
- Molecular Weight:233.1255
826-36-8
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76893-32-8
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Yield:-
Steps:
Multi-step reaction with 6 steps
1.1: acetic acid / 20 °C
1.2: 16 h / 20 °C
2.1: methanol / 6 h / 0 - 20 °C / Inert atmosphere
3.1: 3-chloro-benzenecarboperoxoic acid / diethyl ether / 1.5 h / 0 - 20 °C / Inert atmosphere
4.1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 4.5 h / -78 - -50 °C
5.1: triethylamine / tetrahydrofuran / 1.17 h / 20 °C
6.1: lithium bromide / acetone / 2 h / Reflux
References:
Vuong, Wayne;Mosquera-Guagua, Fabricio;Sanichar, Randy;McDonald, Tyler R.;Ernst, Oliver P.;Wang, Lei;Vederas, John C. [Organic Letters,2019,vol. 21,# 24,p. 10149 - 10153]
76893-27-1
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76893-32-8
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19971-12-1
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76893-32-8
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70473-81-3
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76893-32-8
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55738-75-5
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76893-32-8
13 suppliers
$110.00/2mg