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1,3-Dithiane-2-carboxylic acid, 1,1-dimethylethyl ester synthesis

2synthesis methods
-

Yield:78762-56-8 81%

Reaction Conditions:

with sulfuric acid;magnesium sulfate in dichloromethane; for 18 h;

References:

Zengeya, Thomas T.;Kulkarni, Rhushikesh A.;Meier, Jordan L. [Organic Letters,2015,vol. 17,# 10,p. 2326 - 2329] Location in patent:supporting information