8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine synthesis
- Product Name:8,11-Dichloro-5H-dibenzo[b,e][1,4]diazepine
- CAS Number:50373-22-3
- Molecular formula:C13H8Cl2N2
- Molecular Weight:263.12
![8-Chloro-5,10-dihydrodibenzo[b,e][1,4]diazepin-11-one](/CAS/GIF/50892-62-1.gif)
50892-62-1
190 suppliers
$50.00/1g
50373-22-3
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Yield:50373-22-3 72%
Reaction Conditions:
Stage #1: 8-chloro-5,10-dihydro-11H-dibenzo[b,e][1,4]diazepin-11-onewith N,N-dimethyl-aniline;trichlorophosphate in toluene at 95; for 2 h;
Stage #2: with sodium carbonate in 1,4-dioxane at 80; for 1 h;
References:
Ottesen, Lars K.;Ek, Fredrik;Olsson, Roger [Organic Letters,2006,vol. 8,# 9,p. 1771 - 1773]
67990-66-3
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$38.00/250mg
50373-22-3
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![2-[(4-CHLORO-2-NITROPHENYL)AMINO]-BENZOIC ACID](/CAS/GIF/60091-87-4.gif)
60091-87-4
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50373-22-3
13 suppliers
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118-92-3
0 suppliers
$25.89/25g
50373-22-3
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345-18-6
200 suppliers
$7.00/5g
50373-22-3
13 suppliers
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