8-Acetyl-5,6,7,8-tetrahydroquinoline synthesis
- Product Name:8-Acetyl-5,6,7,8-tetrahydroquinoline
- CAS Number:1146576-61-5
- Molecular formula:C11H13NO
- Molecular Weight:175.23
10500-57-9
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75-05-8
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1146576-61-5
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Yield: 46%
Reaction Conditions:
Stage #1:5,6,7,8-tetrahydroquinoline with n-butyllithium in tetrahydrofuran at 0;Inert atmosphere;
Stage #2:acetonitrile in tetrahydrofuran at 20;Inert atmosphere;
Stage #3: with sulfuric acid;water in tetrahydrofuran
References:
Wang, Deping;Ding, Ke [Chemical Communications,2009,# 14,p. 1891 - 1893] Location in patent:supporting information; experimental part