(S)-METHYL (3,3-DIMETHYL-1-OXO-1-(2-(4-(PYRIDIN-2-YL)BENZYL)HYDRAZINYL)BUTAN-2-YL)CARBAMATE synthesis
- Product Name:(S)-METHYL (3,3-DIMETHYL-1-OXO-1-(2-(4-(PYRIDIN-2-YL)BENZYL)HYDRAZINYL)BUTAN-2-YL)CARBAMATE
- CAS Number:857904-02-0
- Molecular formula:C20H26N4O3
- Molecular Weight:370.45
Yield:857904-02-0 64%
Reaction Conditions:
Stage #1: 4-(2'-pyridyl)benzaldehyde;methyl (S)-(1-hydrazinyl-3,3-dimethyl-1-oxobutan-2-yl)carbamatewith toluene-4-sulfonic acid in tetrahydrofuran at 20; for 1 h;
Stage #2: with sodium cyanoborohydride in tetrahydrofuran at 20;Further stages.;
References:
Wu, Xiongyu;?hrngren, Per;Ekegren, Jenny K.;Unge, Johan;Unge, Torsten;Wallberg, Hans;Samuelsson, Bertil;Hallberg, Anders;Larhed, Mats [Journal of Medicinal Chemistry,2008,vol. 51,# 4,p. 1053 - 1057]
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