7-benzyl-4-chloro-2-(methylthio)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine synthesis
- Product Name:7-benzyl-4-chloro-2-(methylthio)-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine
- CAS Number:859826-11-2
- Molecular formula:C15H16ClN3S
- Molecular Weight:305.83
52763-21-0
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sodium methylate / methanol / 16 h / 100 °C / Sealed tube
1.2: 1 h / 20 °C
2.1: trichlorophosphate; N,N-dimethyl-aniline / 1,2-dichloro-ethane / 90 °C
References:
Cadent Therapeutics, Inc.;Jefson, Martin R.;Keaney, Gregg F.;Larsen, Janus Schreiber;Lowe, III, John A.;McCall, John M. US2017/355708, 2017, A1
![Pyrido[3,4-d]pyrimidin-4(4aH)-one, 5,6,7,8-tetrahydro-2-(methylthio)-7-(phenylmethyl)-](/CAS/20200515/GIF/871107-81-2.gif)
871107-81-2
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859826-11-2
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39514-19-7
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