(1R,2S)-2-[[(1,1-Dimethylethoxy)carbonyl]amino]cyclobutanecarboxylic acid synthesis
- Product Name:(1R,2S)-2-[[(1,1-Dimethylethoxy)carbonyl]amino]cyclobutanecarboxylic acid
- CAS Number:868364-63-0
- Molecular formula:C10H17NO4
- Molecular Weight:215.25
88335-88-0
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: chloroformic acid ethyl ester; triethylamine / acetone / 0.5 h / 0 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: toluene / 12 h / Reflux
3.1: sodium hydroxide / tetrahydrofuran; water / 3 h / 0 °C
References:
Sans, Marta;Illa, Ona;Ortuno, Rosa M. [Organic Letters,2012,vol. 14,# 10,p. 2431 - 2433]
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