(3,5-Bis(tridecafluorohexyl)phenyl)diphenylphosphane synthesis
- Product Name:(3,5-Bis(tridecafluorohexyl)phenyl)diphenylphosphane
- CAS Number:874161-77-0
- Molecular formula:C30H13F26P
- Molecular Weight:898.36
355-43-1
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: 32 percent / copper powder / dimethylsulfoxide / 16 h / 120 °C
2.1: n-BuLi / hexane; diethyl ether / 4 h / -78 °C
2.2: hexane; diethyl ether / -78 - 20 °C
References:
Adams, Dave J.;Bennett, James A.;Cole-Hamilton, David J.;Hope, Eric G.;Hopewell, Jonathan;Kight, Jo;Pogorzelec, Peter;Stuart, Alison M. [Dalton Transactions,2005,# 24,p. 3862 - 3867]
626-39-1
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