9,9-Di-n-octylfluorene-2,7-dicarboxaldehyde synthesis
- Product Name:9,9-Di-n-octylfluorene-2,7-dicarboxaldehyde
- CAS Number:380600-91-9
- Molecular formula:C31H42O2
- Molecular Weight:446.66
16433-88-8
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380600-91-9
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: potassium iodide; potassium hydroxide / dimethyl sulfoxide / 24 h / 20 °C
2.1: tert.-butyl lithium / tetrahydrofuran; pentane / 1 h / -78 °C / Inert atmosphere
2.2: 2 h / -78 - 20 °C / Inert atmosphere
3.1: manganese(IV) oxide / benzene / Dean-Stark; Reflux
References:
Intemann, Jeremy J.;Mike, Jared F.;Cai, Min;Barnes, Charles A.;Xiao, Teng;Roggers, Robert A.;Shinar, Joseph;Shinar, Ruth;Jeffries-El, Malika [Journal of Polymer Science, Part A: Polymer Chemistry,2013,vol. 51,# 4,p. 916 - 923]
222159-97-9
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380600-91-9
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198964-46-4
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86-73-7
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111-83-1
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380600-91-9
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