9-Oxabicyclo[6.1.0]nonan-4-one(8CI,9CI) synthesis

3synthesis methods

Product Name:9-Oxabicyclo[6.1.0]nonan-4-one(8CI,9CI)
CAS Number:28399-88-4
Molecular formula:C8H12O2
Molecular Weight:0

111-78-4
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: 59 percent / 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 4 h / Ambient temperature
2: 70 percent / LiAlH₄ / diethyl ether / 24 h / Heating
3: 62 percent / Jones-reagent / acetone / Ambient temperature
4: 88 percent / 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / Ambient temperature

References:

Meier, Herbert;Mayer, Winfried;Kolshorn, Heinz [Chemische Berichte,1987,vol. 120,p. 685 - 690]

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28399-88-4
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References

4277-34-3 Synthesis

4277-34-3
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References