(2-fluoro-6-iodophenyl)carbaMic acid tert-butyl ester synthesis
- Product Name:(2-fluoro-6-iodophenyl)carbaMic acid tert-butyl ester
- CAS Number:908600-92-0
- Molecular formula:C11H13FINO2
- Molecular Weight:337.1293
98968-72-0
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$30.00/250mg
908600-92-0
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Yield:908600-92-0 79%
Reaction Conditions:
Stage #1: tert-butyl 2-fluorophenylcarbamatewith carbon dioxide;tert.-butyl lithium in tetrahydrofuran;pentane at -78 - -20; for 1.5 h;
Stage #2: with iodine in tetrahydrofuran;pentane at 20;Further stages.;
References:
Jensen, Thomas;Pedersen, Henrik;Bang-Andersen, Benny;Madsen, Robert;Jorgensen, Morten [Angewandte Chemie - International Edition,2008,vol. 47,# 5,p. 888 - 890]
886762-73-8
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$22.00/100mg
24424-99-5
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$13.50/25G
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348-54-9
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$10.00/1g
908600-92-0
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24424-99-5
869 suppliers
$13.50/25G
908600-92-0
5 suppliers
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