tert-butyl 7-formyl-3,4-dihydro-1,8-naphthyridine-1(2H)-carboxylate synthesis

3synthesis methods

Product Name:tert-butyl 7-formyl-3,4-dihydro-1,8-naphthyridine-1(2H)-carboxylate
CAS Number:912270-39-4
Molecular formula:C14H18N2O3
Molecular Weight:262.3

445490-78-8 Synthesis

1-BOC-7-(2-HYDROXYETHYL)-3,4-DIHYDRO-1,8-NAPHTHYRIDINE

445490-78-8
30 suppliers
$295.00/0.25 / G

tert-butyl 7-formyl-3,4-dihydro-1,8-naphthyridine-1(2H)-carboxylate

912270-39-4
16 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 89 percent / I₂; imidazole; triethylamine / triphenylphosphine / CH₂Cl₂ / 0 - 25 °C
2: 53 percent / potassium tert-butoxide / tetrahydrofuran / -78 - 20 °C
3: 57 percent / sodium periodate; 4-methylmorpholine-N-oxide; OsO₄ / acetonitrile; H₂O / 20 °C

References:

Raboisson, Pierre;DesJarlais, Renee L.;Reed, Rolanda;Lattanze, Jennifer;Chaikin, Margery;Manthey, Carl L.;Tomczuk, Bruce E.;Marugan, Juan Jose [European Journal of Medicinal Chemistry,2007,vol. 42,# 3,p. 334 - 343]

1,8-Naphthyridine-1(2H)-carboxylic acid, 7-ethenyl-3,4-dihydro-, 1,1-dimethylethyl ester

912270-30-5
0 suppliers
inquiry

912270-39-4
16 suppliers
inquiry

References

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

912270-39-4
16 suppliers
inquiry

References

HomePage | About Us | Member Companies | Advertising | Contact us | Previous WebSite | MSDS | CAS Index | CAS DataBase | Product Catalog | Links | Privacy | Terms | Product Manufacturers | New Products
All products displayed on this website are only for non-medical purposes such as industrial applications or scientific research, and cannot be used for clinical diagnosis or treatment of humans or animals. They are not medicinal or edible.
According to relevant laws and regulations and the regulations of this website, units or individuals who purchase hazardous materials should obtain valid qualifications and qualification conditions.