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p-Nitrobenzyl 2-Diazo-3-trimethylsilyloxy-3-butenoate synthesis

4synthesis methods
27607-77-8 Synthesis
Trimethylsilyl trifluoromethanesulfonate

27607-77-8
485 suppliers
$10.00/5g

82551-63-1 Synthesis
4-Nitrobenzyl 2-diazoacetoacetate

82551-63-1
157 suppliers
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p-Nitrobenzyl 2-Diazo-3-trimethylsilyloxy-3-butenoate

93788-47-7
2 suppliers
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Yield:93788-47-7 90%

Reaction Conditions:

with triethylamine in dichloromethane at 0 - 5; for 0.5 h;

References:

Ueda;Roberge;Vinet [Canadian Journal of Chemistry,1984,vol. 62,# 12,p. 2936 - 2940]