Methyl 4-chloro-1H-pyrrolo[2,3-b]pyridine-5-carboxylate synthesis
- Product Name:Methyl 4-chloro-1H-pyrrolo[2,3-b]pyridine-5-carboxylate
- CAS Number:951625-93-7
- Molecular formula:C9H7ClN2O2
- Molecular Weight:210.62
55052-28-3
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951625-93-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C
1.2: 20 °C
2.1: sec.-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: 0.5 h / -78 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
References:
SANFORD-BURNHAM MEDICAL RESEARCH INSTITUTE;PINKERTON, Anthony, B.;HASSIG, Christian, A.;JACKSON, Michael, R.;ARDECKY, Robert, John;PASS, Ian WO2016/123392, 2016, A2
67-56-1
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![1H-Pyrrolo[2,3-b]pyridine-5-carboxylic acid, 4-chloro-](/CAS/GIF/920966-03-6.gif)
920966-03-6
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951625-93-7
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![1H-Pyrrolo[2,3-b]pyridine, 4-chloro-1-[tris(1-methylethyl)silyl]-](/CAS/GIF/651744-48-8.gif)
651744-48-8
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$225.00/1 g
951625-93-7
77 suppliers
$45.00/1g