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17167-73-6

Acetaldehyde methyl hydrazone synthesis

5synthesis methods
-

Yield:17167-73-6 0.02 g ,3530-13-0 0.022 g

Reaction Conditions:

Stage #1: acetylacetonewith ferrocenecarboxaldehyde;piperdinium acetate in benzene;Knoevenagel condensation;
Stage #2: methylhydrazine in ethanol at 20; for 18 h;Inert atmosphere;

References:

Klimova, Elena I.;Vazquez Lopez, Eduardo A.;Martinez Mendoza, Juan M.;Ramirez, Lena Ruiz;Alamo, Marcos Flores;Backinowsky, Leon V. [Journal of Heterocyclic Chemistry,2009,vol. 46,# 3,p. 484 - 491] Location in patent:experimental part