ADIPIC ACID MONOBENZYL ESTER synthesis
- Product Name:ADIPIC ACID MONOBENZYL ESTER
- CAS Number:40542-90-3
- Molecular formula:C13H16O4
- Molecular Weight:236.26
124-04-9
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40542-90-3
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Yield: 87%
Reaction Conditions:
with DOWEX 50W-X2 in octane at 100; for 4 h;Heating / reflux;
Steps:
12
DOWEX 50W-X2 (2 g), benzyl formate (10 mL, mol), and adipic acid (2 g, mol) were added to octane (10 mL). The mixture was refluxed for 4 hours at 100° C., and the crude product was purified via silica chromatography to yield a clear, colorless liquid (87% yield). 1H NMR (CDCl3) 1.59-1.78 (m, 4H, CH2CH2), 2.33-2.39 (m, 4H, CH2COOH), 5.09 (s, 2H, PhCH2), 7.25-7.30 (m, 5H, aromatic).
References:
Colson, Yolonda;Azouz, Solomon;Grinstaff, Mark;Wolinsky, Jesse;Griset, Aaron US2008/75718, 2008, A1 Location in patent:Page/Page column 41
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40542-90-3
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78277-26-6
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40542-90-3
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124-04-9
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40542-90-3
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