Benzyl formate synthesis
- Product Name:Benzyl formate
- CAS Number:104-57-4
- Molecular formula:C8H8O2
- Molecular Weight:136.15
64-18-6
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100-51-6
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104-57-4
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$6.00/25g
Yield:104-57-4 98%
Reaction Conditions:
with tribromo-isocyanuric acid in neat (no solvent) at 20; for 0.0833333 h;
Steps:
Formylation of benzyl alcohol using formic acidcatalyzed by tribromoisocyanuric acid
To a mixture of the benzyl alcohol (1 mmol)and formic acid (3 mmol); 0.1 g tribromoisocyanuricacid (0.3 mmol) was added. The reaction mixturewas stirred at room temperature for 5 min. Aftercompletion of the reaction (TLC), dichloromethane(10 mL) was added to the reaction mixture andfiltered. The product was extracted with H2O (3×10mL), and the organic layer was dried over anhydrousNa2SO4salt. Evaporation of the solvent underreduced pressure to give the almost pure product.
References:
Hekmatian, Zahra;Khazaei, Ardeshir [Oriental Journal of Chemistry,2015,vol. 31,# 3,p. 1565 - 1570]
100-51-6
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109-94-4
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104-57-4
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107-31-3
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100-51-6
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104-57-4
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93-61-8
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100-51-6
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104-57-4
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100-44-7
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64-18-6
1054 suppliers
$22.12/250ML
100-44-7
623 suppliers
$13.50/250G
104-57-4
244 suppliers
$6.00/25g