AKOS B013937 synthesis
- Product Name:AKOS B013937
- CAS Number:17431-97-9
- Molecular formula:C10H11NO5
- Molecular Weight:225.2
Yield:17431-97-9 62.8%
Reaction Conditions:
Stage #1: ethyl 2-bromoisobutyrate;4-nitro-phenolwith potassium carbonate in acetonitrile; for 8 h;Reflux;
Stage #2: with lithium hydroxide in tetrahydrofuran;methanol;water at 20; for 3 h;
Stage #3: with hydrogenchloride in tetrahydrofuran;methanol;water;
References:
Almanza-Pérez, Julio Cesar;Chávez-Silva, Fabiola;Colin-Lozano, Blanca;Estrada-Soto, Samuel;Hidalgo-Figueroa, Sergio;Navarrete-Vazquez, Gabriel;Torres-Gomez, Héctor [Pharmaceuticals,2022,vol. 15,# 1,art. no. 102]
100-02-7
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$11.00/5G
67-66-3
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$33.60/500ml
67-64-1
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$19.10/10ml
17431-97-9
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23501-39-5
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17431-97-9
21 suppliers
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100-02-7
36 suppliers
$11.00/5G
17431-97-9
21 suppliers
inquiry