Benzene, 1,3-bis(1,1-dimethylethyl)-5-iodo- synthesis
- Product Name:Benzene, 1,3-bis(1,1-dimethylethyl)-5-iodo-
- CAS Number:37055-53-1
- Molecular formula:C14H21I
- Molecular Weight:316.22
Yield: 63.9 %Chromat.
Reaction Conditions:
with trifluoroacetic acid at 20; for 0.166667 h;
Steps:
Compound II, 0.162 g (0.25 mmol), was added to a solution of 0.247 g (1 mmol) of I in 5 ml of trifluoroacetic acid, and the mixture was stirred for 10 min at 20°C.
References:
Nguen, M.;Chaikovskii, V. K.;Filimonov, V. D.;Funk, A. A. [Russian Journal of Organic Chemistry,2012,vol. 48,# 6,p. 780 - 782,3]
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