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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
939-37-7

Benzene, 1,3-dimethyl-5-(1-methylpropyl)- synthesis

6synthesis methods
Einecs 208-163-1

52152-71-3
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22445-41-6 Synthesis
1-Iodo-3,5-dimethylbenzene

22445-41-6
202 suppliers
$5.00/5g

Benzene, 1,3-dimethyl-5-(1-methylpropyl)-

939-37-7
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Yield:939-37-7 92%

Reaction Conditions:

Stage #1: 2-butyl iodidewith zinc in tetrahydrofuran at 20;Inert atmosphere;
Stage #2: 3,5-dimethylphenyl iodidewith 2,2':6,2''-terpyridine;nickel dichloride in tetrahydrofuran at 40; for 17 h;Inert atmosphere;Negishi coupling reaction;

References:

Joshi-Pangu, Amruta;Ganesh, Madhu;Biscoe, Mark R. [Organic Letters,2011,vol. 13,# 5,p. 1218 - 1221] Location in patent:supporting information; experimental part

5-Bromo-m-xylene

556-96-7
382 suppliers
$6.00/5g

1-Aza-5-stannabicyclo[3.3.3]undecane, 5-(1-methylpropyl)-

142509-27-1
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Benzene, 1,3-dimethyl-5-(1-methylpropyl)-

939-37-7
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References
(±)-sec-Butyl chloride

53178-20-4
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Aluminum

7429-90-5
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$9.00/5g

Benzene, 1,3-dimethyl-5-(1-methylpropyl)-

939-37-7
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References
Benzene, 1-butyl-2,4-dimethyl-

1601-73-6
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Benzene, 1,3-dimethyl-5-(1-methylpropyl)-

939-37-7
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References
Benzo[b]thiophene, 2,3,5,7-tetramethyl-

1011-02-5
1 suppliers
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Benzene, 1,3-dimethyl-5-(1-methylpropyl)-

939-37-7
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References