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ChemicalBook CAS DataBase List Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI)
731772-97-7

Benzene, 1-fluoro-2-(2-methyl-2-propenyl)- (9CI) synthesis

1synthesis methods
-

Yield:731772-97-7 43%

Reaction Conditions:

with di-tert-butyl(2-methoxyphenyl)phosphine;palladium diacetate;silver pivalate;caesium carbonate in neat (no solvent) at 120; for 17 h;Inert atmosphere;Sealed tube;regioselective reaction;

References:

Lee, Sarah Yunmi;Hartwig, John F. [Journal of the American Chemical Society,2016,vol. 138,# 46,p. 15278 - 15284] Location in patent:supporting information