Benzene, 2,3-dimethoxy-1,4-bis(trimethylsilyl)- synthesis
- Product Name:Benzene, 2,3-dimethoxy-1,4-bis(trimethylsilyl)-
- CAS Number:92669-92-6
- Molecular formula:C14 H26 O2 Si2
- Molecular Weight:282.53
Yield:92669-92-6 89%
Reaction Conditions:
Stage #1: (2,3-dimethoxyphenyl)trimethylsilanewith n-butyllithium;N,N,N,N,-tetramethylethylenediamine in hexane at 20; for 25 h;
Stage #2: chloro-trimethyl-silane in hexane at -78 - 20; for 5 h;Further stages.;
References:
Zhu, Zhengguo;Swager, Timothy M. [Organic Letters,2001,vol. 3,# 22,p. 3471 - 3474]
91-16-7
591 suppliers
$13.00/25g
92669-92-6
1 suppliers
inquiry
75-77-4
594 suppliers
$5.04/10
91-16-7
591 suppliers
$13.00/25g
92669-91-5
2 suppliers
inquiry
92669-92-6
1 suppliers
inquiry