Benzene, 2-ethenyl-1,4-diMethoxy- synthesis
- Product Name:Benzene, 2-ethenyl-1,4-diMethoxy-
- CAS Number:14568-68-4
- Molecular formula:C10H12O2
- Molecular Weight:164.2
Yield:14568-68-4 93%
Reaction Conditions:
Stage #1: Methyltriphenylphosphonium bromidewith sodium amide in diethyl ether at 20; for 10 h;Inert atmosphere;
Stage #2: 2,5-dimethoxybenzaldehyde in diethyl ether at -10 - 20;Inert atmosphere;Wittig reaction;
References:
Sun, Bin;Hoshino, Juma;Jermihov, Katie;Marler, Laura;Pezzuto, John M.;Mesecar, Andrew D.;Cushman, Mark [Bioorganic and Medicinal Chemistry,2010,vol. 18,# 14,p. 5352 - 5366] Location in patent:experimental part
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