BenzeneMethanol, 3-Methoxy-4-Methyl- synthesis

8synthesis methods

Product Name:BenzeneMethanol, 3-Methoxy-4-Methyl-
CAS Number:4685-50-1
Molecular formula:C9H12O2
Molecular Weight:152.19

3556-83-0 Synthesis

3556-83-0
152 suppliers
$7.00/1g

4685-50-1
27 suppliers
$110.00/0.5g

Yield:4685-50-1 100%

Reaction Conditions:

with lithium aluminium tetrahydride in tetrahydrofuran at 0; for 0.5 h;

Steps:

2.35

Example 2.35: 3-(3-methoxy-4-methylphenyl)propan-l-amine; [0277] To methyl 3-methoxy-4-methylbenzoate (3gm, 16.6 mmol) in THF (60 ml) at O⁰C, LAH (3gm, 66.6 mmol) was slowly added. After stirring at O⁰C for further 30 min, reaction mixture was worked up as described above to obtain the alcohol (3-methoxy-4- methylphenyl)methanol in quantitative yield.

References:

WO2006/110668,2006,A1 Location in patent:Page/Page column 65

7151-68-0 Synthesis