3-METHOXY-4-METHYLBENZALDEHYDE synthesis
- Product Name:3-METHOXY-4-METHYLBENZALDEHYDE
- CAS Number:24973-22-6
- Molecular formula:C9H10O2
- Molecular Weight:150.17
4685-50-1
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$110.00/0.5g
24973-22-6
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$6.00/100mg
Yield: 100%
Reaction Conditions:
with Dess-Martin periodane in dichloromethane at 0; for 0.5 h;
Steps:
2.35
Dess-Martin periodinane (3gm, 7.07 mmol) was added to (3-methoxy-4- methylphenyl)methanol (lgm, 6.57 mmol) in CH2Cl2 (35 ml) at O0C. After stirring at O0C for 0.5h, some of the CH2Cl2 was removed, reaction mixture was diluted with ether, washed with sodium bicarbonate solution, sodium thiosulfate solution and water. Organic layer was dried and evaporated to obtain 3-methoxy-4-methylbenzaldehyde in quantitative yield.
References:
ZAPAQ, INC.;THE BOARD OF TRUSTEES OF THE UNVERSITY OF ILLINOIS;OKLAHOMA MEDICAL RESEARCH FOUNDATION WO2006/110668, 2006, A1 Location in patent:Page/Page column 65
57295-30-4
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74-88-4
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24973-22-6
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108-48-5
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87808-44-4
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24973-22-6
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591-31-1
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$10.00/5g
74-88-4
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$15.00/10g
24973-22-6
113 suppliers
$6.00/100mg
57295-30-4
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$131.00/250mg
77-78-1
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$19.69/1ml
24973-22-6
113 suppliers
$6.00/100mg