Benzo[j]phenanthridin-6(5H)-one synthesis
- Product Name:Benzo[j]phenanthridin-6(5H)-one
- CAS Number:2413-02-7
- Molecular formula:C17H11NO
- Molecular Weight:245.28
93-09-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: thionyl chloride; magnesium sulfate / 1,2-dichloro-benzene / 24 h / 120 °C / Inert atmosphere
2: silver(l) oxide; potassium carbonate; palladium diacetate; acetic acid / 24 h / 130 °C / Inert atmosphere
3: palladium dichloride; copper diacetate; oxygen / dimethyl sulfoxide / 160 °C
References:
Large, Benjamin;Gigant, Nicolas;Joseph, Delphine;Clavier, Gilles;Prim, Damien [European Journal of Organic Chemistry,2019,vol. 2019,# 8,p. 1835 - 1841]
20717-80-0
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