Benzonitrile, 4-acetyl-2-methoxy- synthesis
- Product Name:Benzonitrile, 4-acetyl-2-methoxy-
- CAS Number:102362-02-7
- Molecular formula:C10H9NO2
- Molecular Weight:175.18
2486-69-3
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$8.00/1g
102362-02-7
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 1.) NaNO2, conc. HCl / 1.) H2O, 0-5 deg C, 1 h, 2.a) 50 deg C, 2.b) 2 h, reflux
2: SOCl2 / toluene / 3 h / Heating
3: 1.) THF, ether, 0-5 deg C, 1 h, 2.) dioxane, 2 h, reflux
References:
Barraclough;Black;Cambridge;Demaine;Gerskowitch;Giles;Hill;Hull;Lyer;King;Livingstone;Nobbs;Randall;Shah;Whiting [Archiv der Pharmazie,1990,vol. 323,# 8,p. 507 - 512]
330793-38-9
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111-34-2
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$13.00/25mL
102362-02-7
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75-86-5
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$80.00/5g
1131-62-0
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$14.00/5g
113016-89-0
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102362-02-7
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22106-40-7
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$55.00/50 mg
102362-02-7
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102362-00-5
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102362-02-7
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