BENZYL 3-(CHLOROSULFONYL)PIPERIDINE-1-CARBOXYLATE synthesis
- Product Name:BENZYL 3-(CHLOROSULFONYL)PIPERIDINE-1-CARBOXYLATE
- CAS Number:1311317-42-6
- Molecular formula:C13H16ClNO4S
- Molecular Weight:317.79
912369-01-8
0 suppliers
inquiry
1311317-42-6
16 suppliers
$285.00/100mg
Yield:-
Reaction Conditions:
with water;chlorine in dichloromethane at 0; for 3.5 h;
Steps:
6.3 Step 3 : benzyl 3-(chlorosulfonyl)piperidine-l-carboxylate
To a solution of Compound 6-3 (2.1 g, 7.15 mmol, 1.0 eq) in CH2CI2 (40 mL) was added water (8 mL) at 0°C and the reaction mixture was bubbled through chlorine gas for 3.5 hours. TLC (petroleum ether/EtOAc 5: 1) showed most of Compound 6-3 was consumed. The organic layer was separated and dried over Na SO . filtered. The filtrate was used for the next step directly as a solution.
References:
WO2020/58913,2020,A1 Location in patent:Page/Page column 51-52
169750-63-4
3 suppliers
inquiry
1311317-42-6
16 suppliers
$285.00/100mg
95798-22-4
107 suppliers
$11.00/1g
1311317-42-6
16 suppliers
$285.00/100mg
6859-99-0
407 suppliers
$6.00/5g
1311317-42-6
16 suppliers
$285.00/100mg
501-53-1
409 suppliers
$10.00/1g
1311317-42-6
16 suppliers
$285.00/100mg