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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide
ChemicalBook CAS DataBase List BETA-(2-THIENYL)-DL-ALANINE
2021-58-1

BETA-(2-THIENYL)-DL-ALANINE synthesis

4synthesis methods
98-03-3 Synthesis
2-Thiophenecarboxaldehyde

98-03-3
553 suppliers
$5.00/25g

BETA-(2-THIENYL)-DL-ALANINE

2021-58-1
103 suppliers
$30.00/1G

-

Yield:-

Steps:

Multi-step reaction with 6 steps
1.1: NaBH4 / methanol / 20 °C
2.1: SOCl2; benzotriazole / CH2Cl2
3.1: NaH / dimethylformamide; various solvent(s) / 0.5 h / 20 °C
3.2: 82 percent / dimethylformamide; various solvent(s) / 7 h / 20 - 60 °C
4.1: NaOH / methanol / 20 h / 20 °C
5.1: toluene / 2 h / Heating
6.1: 75 percent / aq. LiOH / 2.5 h / 60 °C

References:

Paizs, Csaba;Katona, Adrian;Retey, Janos [Chemistry - A European Journal,2006,vol. 12,# 10,p. 2739 - 2744]

FullText

765-50-4 Synthesis
2-(Chloromethyl)thiophene

765-50-4
101 suppliers
$166.94/1G

BETA-(2-THIENYL)-DL-ALANINE

2021-58-1
103 suppliers
$30.00/1G

References
636-72-6 Synthesis
2-Thiophenemethanol

636-72-6
258 suppliers
$6.00/5g

BETA-(2-THIENYL)-DL-ALANINE

2021-58-1
103 suppliers
$30.00/1G

References
2-Thiophenepropanoicacid, a-thioxo-

89677-36-1
0 suppliers
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BETA-(2-THIENYL)-DL-ALANINE

2021-58-1
103 suppliers
$30.00/1G

References

BETA-(2-THIENYL)-DL-ALANINE Related Search:

D-2-THIENYLALANINE L-3-Pyridylalanine L-3-THIENYLALANINE BETA-(2-THIAZOLYL)-DL-ALANINE L-2-THIENYLALANINE L-Alanine BOC-L-2-(5-BROMOTHIENYL)ALANINE BETA-(2-THIENYL)-DL-SERINE Boc-3-(2-thienyl)-L-alanine BOC-D-2-THIENYLALANINE