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beta-C14-Aldehyde synthesis

6synthesis methods
-

Yield:14398-40-4 90%

Reaction Conditions:

with trimethylsilylmethyllithium;lithium bromide in tetrahydrofuran;pentane at -78 - 20;

References:

Pace, Vittorio;Castoldi, Laura;Mazzeo, Eugenia;Rui, Marta;Langer, Thierry;Holzer, Wolfgang [Angewandte Chemie - International Edition,2017,vol. 56,# 41,p. 12677 - 12682][Angew. Chem.,2017,vol. 129,# 41,p. 12851 - 12856,6] Location in patent:supporting information