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BETA-GLUCOSYL YARIV REAGENT synthesis

2synthesis methods
-

Yield:58130-67-9 95%

Reaction Conditions:

Stage #1: 4-aminophenyl β-D-glucopyranosidewith hydrogenchloride;sodium nitrite in water at 0; for 3 h;
Stage #2: 3,5-dihydroxyphenolwith sodium hydroxide pH=Ca. 11;

References:

Hoshing, Raghuraj;Saladino, Michael;Kuhn, Helene;Caianiello, David;Lusi, Robert F.;Basu, Amit [Journal of Organic Chemistry,2020,vol. 85,# 24,p. 16236 - 16242]