Bis(2-methoxyethyl)aminosulfur trifluoride synthesis

2synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1.1: n-BuLi / hexane / -78 - 0 °C
1.2: hexane / 0.5 h / 0 °C
2.1: 2.6 g / diethyl ether / 3 h / -30 - 0 °C

References:

Lal, Gauri S.;Pez, Guido P.;Pesaresi, Reno J.;Prozonic, Frank M.;Cheng, Hansong [Journal of Organic Chemistry,1999,vol. 64,# 19,p. 7048 - 7054]

Bis(2-methoxyethyl)aminosulfur trifluoride Related Search:

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