Bis(3-amino-4-hydroxyphenyl)methanone synthesis
- Product Name:Bis(3-amino-4-hydroxyphenyl)methanone
- CAS Number:22445-98-3
- Molecular formula:C13H12N2O3
- Molecular Weight:244.25
37567-35-4
3 suppliers
inquiry
22445-98-3
4 suppliers
inquiry
Yield:22445-98-3 80.12%
Reaction Conditions:
with palladium 10% on activated carbon;hydrazine hydrate in water at 75; for 6 h;Inert atmosphere;Reagent/catalyst;Temperature;
Steps:
8 Preparation of 4,4'-dihydroxy-3,3'-diaminobenzophenone:
0.01 mol of 4,4'-dihydroxy-3,3'-dinitrobenzophenone in a concentration of 10 wt% Pd / C and 0.556 to 1.667 mol of distilled water were mixed at room temperature and then heated to 60 to 95 ° C, slowly dropping 0.04 ~ 0.11mol hydrazine hydrate, constant temperature reaction 4 ~ 8h, with acid to adjust the pH 1, filter to remove the catalyst, the filtrate by adding alkali precipitation of crystals, and then filter to 4,4'-dihydroxy-3 , 3'-diaminobenzophenone.
References:
CN104478744,2017,B Location in patent:Paragraph 0066; 0067
108-90-7
682 suppliers
$10.00/25G
22445-98-3
4 suppliers
inquiry
122-01-0
384 suppliers
$13.00/25g
22445-98-3
4 suppliers
inquiry
90-98-2
407 suppliers
$27.00/25g
22445-98-3
4 suppliers
inquiry